Some 'bad' GC chromatograms
Nico Vonk
,
Avans+, Breda
,
The Netherlands
Abstract
This chapter shows a series of GC chromatograms with some common problems and their solutions.
Level
Basic
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How to avoid trouble
Diagnosing 'bad' chromatograms
Before you call the service dept!
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The gas system
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Problems when lighting an FID
Some 'bad' GC chromatograms
> Tailing
> Base line drift
> 'Strange' baseline
> Very sharp peaks on the baseline
> 'Poor' peaks
> Poor performance
> Poor chromatogram
> Injection problem? Doubling peaks
> Injection problem
> Disturbed baseline
> Baseline drift
> Poor peakshapes
> Bad performance
> 'Strange' baseline
> 'Ghost peaks'
> Negative peak
> Poor peak shape. Buy new column?
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