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Injection principles of capillary GC
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Injection techniques
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Direct injection
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Manual syringe injection
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Comparison of injectors
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The septum
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Introduction to Capillary GC injection techniques. -
Cold on-column injection
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Cold trapping and solvent effect (A)
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Cold trapping or thermal focussing (A)
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The retention gap
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The retention gap (Animation)
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The PTV injector
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Programmed Temperature Vaporization (PTV) injection -
On-column large volume injection
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Techniques for PTV-LVI
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Optimisation
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LVI using speed controlled sampling
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Thermodesorption
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Headspace analysis
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Dynamic headspace & purge-and-trap
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Liners
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Splitless injection -
Flow control and pressure regulation
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Cold trapping or thermal focussing
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Cold trapping or thermal focussing (A)
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Solvent effect
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Cold trapping and solvent effect (A)
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Split injection -
Introduction
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Method development
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Fundamentals of the hardware
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Basic Operation
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Setting Temperatures and Flows
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What Really Happens in the Glass Liner
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What Really Happens in the Syringe
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Method Development Issues
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Installation of a capillary column to a split injector
